Webbthe CAL standard fails the criteria of Section 10.3, recalibration is in order per Section 10.2. If the CAL standard is acceptable, report results obtained from the reinjected aliquot, but annotate as “suspect/IS recovery.” Alternatively, prepare another aliquot of the sample as specified in Section 11.2 or collect a new sample and re-analyze. WebbWhen I worked in a GMP lab, we would pour bulk solutions from 5L bottles into 100ml-1000ml bottles using funnels. Then any synthesises would use these smaller bottle to pour into graduated cylinders also using funnels. Be sure to label the bottles with who poured it, what it is, and when it was made.
EPA Document #: EPA/600/R-09/149 METHOD 538.
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